Implementation and alignment of a Raman spectroscopy array for powder and liquid samples
A. Quiroz, R. Sánchez
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Base Information
Volume
V50 - N4 / 2017 Ordinario
Reference
417-429
DOI
http://doi.org/10.7149/OPA.50.4.49046
Language
English
Keywords
Raman spectroscopy, optical instrumentation, optical alignment.
Abstract
This paper presents the methodology for the implementation of a conventional Raman spectroscopy array for the qualitative analysis of powder and liquid samples. An alignment methodology has been established for a Raman array with 180° geometry and sample collection on two axes. The array has been optimized to collect Raman signal in the 540 to 700 nm region (Δυ: 160 cm-1 to 4000 cm-1) with integration times of up to 8 seconds without risk of Rayleigh band overlap.
References
BETTY CHUNG, "Control de los contaminantes químicos en el Perú," Scielo, 25, no. 4, (2008) [Online].
Ewen Smith and Geofry Dent, Modern Raman Spectroscopy - A Practical Approach, Primera ed., Antony Rowe and Chippenham Wiltshire, Eds. Chichester, England: John Wiley & Sons, Ltd, (2005).
John Ferraro, Kanzuo Nakamoto, and Chris w. Brown, Introductory Raman Spectroscopy, Segunda ed. California, Estados unidos de America: Academic Press, (2003).
Douglas Skoog, James Holler, and Stanley Crouch, Principios de Análisis Instrumental, sexta ed., Sergio Cervantes Gonzales, Ed. México D.F., México: Cengage, (2008).
Roberto Ysaac Sato Berrú, "Detección de contaminantes en la agricultura mediante espectroscopía Raman," Centro de Investigaciones en óptica, Guanajuato, Tesis de doctorado en ciencias (2003).
Richard Mc. Creery, Raman spectroscopy for chemical analysis, Primera ed. Canadá: Wiley Interscience, (2000).
Paul Clemens, Xin Wei, Bobby L. Wilson, and Renard L. Thomas, "Anatase titanium dioxide coated single wall carbon nanotubes manufactured by sonochemical-hydrothermal technique," Open Journal of Composite materials, 3, pp. 21-32, (2013).
Shuxia Guao, Zuliang Du, and Shuxi Dai, "Analysis of Raman modes in Mn-doped ZnO nanocrystals," Physica status solidi, 246, 10, pp. 2329-2332, (2009).
Florian M. Zehentbauer, Euan J. Bain, and Johannes Kiefer, "Multiple parameter monitoring in a direct methanol fuel cell," Measurement Science and Technology, 23, 045602 (2012).
Constanca Cacela, M.L. Duarte, and Rui Fausto, "Structural and vibrational characterisation of 3-amino-1-propanol a concerted SCF-MO ab initio, Raman and infrared (matrix isolation and liquid phase) spectroscopy study," Spectrochimica Acta Part A, 56, pp. 1051-1064, (2000).
ChemicalBooks. [Online].